Cat.NO.:A678231 Purity:98%
Product Details of [ 100-60-7 ]
| CAS No. : | 100-60-7 |
| Formula : |
C7H15N |
| M.W : |
113.20
|
| SMILES Code : | CNC1CCCCC1 |
| MDL No. : | MFCD00003832 |
| InChI Key : | XTUVJUMINZSXGF-UHFFFAOYSA-N |
| Pubchem ID : | 7514 |
Safety of [ 100-60-7 ]
| GHS Pictogram: |    |
| Signal Word: | Danger |
| Hazard Statements: | H226-H302+H332-H314 |
| Precautionary Statements: | P261-P270-P240-P210-P233-P243-P241-P242-P271-P264-P280-P370+P378-P303+P361+P353-P301+P330+P331-P363-P301+P312+P330-P304+P340+P310-P305+P351+P338+P310-P403+P235-P405-P501 |
| Class: | 8(3) |
| UN#: | 2734 |
| Packing Group: | Ⅱ |
Application In Synthesis of [ 100-60-7 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 100-60-7 ]
[ 100-60-7 ] Synthesis Path-Downstream 1~4
- 1
[ 100-60-7 ]
[ 3034-48-8 ]
[ 21166-13-2 ]
- 2
- [ 100-60-7 ]
- [ 3034-48-8 ]
- [ 21166-12-1 ]
- 3
- [ 100-60-7 ]
[ 1227934-69-1 ]
[ 1227934-71-5 ]- [ 1227934-99-7 ]
| Yield | Reaction Conditions | Operation in experiment |
|---|---|---|
| 2-(cyclohexyl(methyl)amino)-4-trifluoromethyloxazole-5-carboxylic Acid (A-34) Intermediate A-34 was prepared by the general procedure for intermediate A-4, by using A-2 and N-methylcyclohexylamine as starting materials. MS (M+1): 293. |
References: [1]Patent: US2011/224137,2011,A1 .
- 4
- [ 100-60-7 ]
[ 161957-56-8 ]- 3-bromo-N-cyclohexyl-2-fluoro-N-methyl-benzamide [ No CAS ]
| Yield | Reaction Conditions | Operation in experiment |
|---|---|---|
| With N-ethyl-N,N-diisopropylamine; HATU; In dichloromethane; for 3h; | 5a) 3-Bromo-N-cyclohexyl-2-fluoro-N-methyl-benzamide A solution of 3-bromo-2-fluoro-benzoic acid (0.50 g, 2.28 mmol), HATU (0.868 g, 2.28 mmol), N-cyclohexyl-N-methylamine (0.297 g, 2.63 mmol) and DIPEA (0.590 g, 4.57 mmol) in DCM (15 mL) was stirred for 3 h. The mixture was washed with aqueous NaHC03 and dried by passage through a phase separation cartridge. Concentration to dryness gave the crude product (0.905 g, quantative), used without further purification. LC-MS m/z 314 (M + H) +, 1 .50 (ret. time). |
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